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HRID1090281

反应详情

EQUATION

反应方程式

HRID 1090281 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)C(C)(C)CC(=O)CSc1ccccc1C(C)C
HCID15035419

未命名化合物

结构：CC(C)c1ccc(N(N)Cc2ccc(Cl)cc2)cc1.Cl
HCID19752394

1-[(4-Chlorophenyl)methyl]-1-[4-(propan-2-yl)phenyl]hydrazine--hydrogen chloride (1/1)

C16H20Cl2N2

PRODUCTS

生成物

1
结构：CC(C)c1ccc2c(c1)c(Sc1ccccc1C(C)C)c(CC(C)(C)C(=O)O)n2Cc1ccc(Cl)cc1
HCID15035402

未命名化合物

PROCEDURE

实验过程

Following the procedure of Example 104, but using 1-(p-chlorobenzyl)-1-[4-(i-propyl)phenyl]hydrazine hydrochloride and methyl 2,2-dimethyl-4-oxo-5-(2-isopropylphenylthio)pentanoate as starting materials followed by hydrolysis at reflux gave the title compound, m.p. 142°-143°.

WORKUP

后处理

  1. customfollowed by hydrolysis
  2. temperatureat reflux