HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropylamine → HCID 19915076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropylamine | HCID 6363 | — |
| Reactant | Bispyribac | HCID 443031 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19915076 | HCID 19915076 | — |
Reaction Steps
2,6-bis[(4,6-dimethoxypyrimidin-2-yl)oxy]benzoic acid (2.0 g) and isopropylamine (1.0 g) were dissolved in 30 ml of THF, and the mixture was stirred at room temperature for 12 hours. The reaction solution was concentrated, and crystals thereby precipitated, were washed with hexane to obtain the above identified compound as white crystals (1.9 g). (Melting point: 99-102° C.)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05081244 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-f8ab7b28e7d34fb5b1c014d6b66773b5 |
| Source note | uspto-grants-1992_01 |