1-Bromopentane → HCID 15599405, compound

HRID 1090309Notes

Reaction equation

HRID 1090309 reaction equation
[CH3:1][S:2]([N:5]1[C:10]2[CH:11]=[C:12]([C:15]3[CH2:16][CH2:17][C:18](=[O:21])[NH:19][N:20]=3)[CH:13]=[CH:14][C:9]=2[O:8][CH2:7][CH2:6]1)(=[O:4])=[O:3].[CH2:22](Br)[CH2:23][CH2:24][CH2:25][CH3:26]>>[CH3:1][S:2]([N:5]1[C:10]2[CH:11]=[C:12]([C:15]3[CH2:16][CH2:17][C:18](=[O:21])[N:19]([CH2:22][CH2:23][CH2:24][CH2:25][CH3:26])[N:20]=3)[CH:13]=[CH:14][C:9]=2[O:8][CH2:7][CH2:6]1)(=[O:4])=[O:3]

Participants

3

Reactant 2

HCID 80571-BromopentaneHCID 14230055HCID 14230055, compound

Product 1

HCID 15599405HCID 15599405, compound

Procedure

6-(3,4-Dihydro-4-methanesulfonyl-1,4(2H)-benzoxazin-6-yl)-2,3,4,5-tetrahydropyridazin-3-one was reacted with pentyl bromide in place of methyl iodide following the procedure of Example 9. The title compound was recovered, yield 1.46 g, mp 138°-139° C.

Workup

  1. customThe title compound was recovered

Sources & evidence

ORD record
ord-3d71ad3ffffe4a28a74b5e8a3c163f89
Source dataset
uspto-grants-1992_01
Patent number
US05081242

Reaction notes

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