Acrylonitrile → HCID 14419663, compound

HRID 1090356Notes

Reaction equation

HRID 1090356 reaction equation
[C:1](#[N:4])[CH:2]=[CH2:3].[CH2:5]([O:9][CH:10]([O:13][CH2:14][CH2:15][CH2:16][CH3:17])[CH:11]=[O:12])[CH2:6][CH2:7][CH3:8]>C(O)CCC>[C:1]([C:2]([CH:11]([OH:12])[CH:10]([O:9][CH2:5][CH2:6][CH2:7][CH3:8])[O:13][CH2:14][CH2:15][CH2:16][CH3:17])=[CH2:3])#[N:4]

Participants

4

Reactant 2

HCID 7855AcrylonitrileHCID 11084609HCID 11084609, compound

Product 1

HCID 14419663HCID 14419663, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

0.17 mole acrylonitrile and 30 g (0.15 mole) of 95.5% by weight dibutoxyethanal in butanol were reacted using the method of example 1 to form 22 g of 2-cyano-4,4-dibutoxy-3-hydroxy-1-butene which distilled at 108° C. under 0.1 mbar.

Sources & evidence

ORD record
ord-f8f604bc3bdd4f9b80453b29cd4f2a29
Source dataset
uspto-grants-1992_01
Patent number
US05081276

Reaction notes

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