Butyl Acrylate → HCID 14419665, compound

HRID 1090358Notes

Reaction equation

HRID 1090358 reaction equation
[C:1]([O:5][CH2:6][CH2:7][CH2:8][CH3:9])(=[O:4])[CH:2]=[CH2:3].[CH2:10]([O:14][CH:15]([O:18][CH2:19][CH2:20][CH2:21][CH3:22])[CH:16]=[O:17])[CH2:11][CH2:12][CH3:13]>C(O)CCC>[CH2:6]([O:5][C:1]([C:2]([CH:16]([OH:17])[CH:15]([O:14][CH2:10][CH2:11][CH2:12][CH3:13])[O:18][CH2:19][CH2:20][CH2:21][CH3:22])=[CH2:3])=[O:4])[CH2:7][CH2:8][CH3:9]

Participants

4

Reactant 2

HCID 8846Butyl AcrylateHCID 11084609HCID 11084609, compound

Product 1

HCID 14419665HCID 14419665, compound

Reagents, catalysts & solvents 1

HCID 2631-ButanolSolvent

Procedure

0.4 moles butyl acrylate and 70 g (0.355 mole) of 95.5% by weight dibutoxyethanal in butanol were reacted using the method of example 1 to form 2-butoxycarbonyl-4,4-dibutoxy-3-hydroxy-1-butene as a colourless liquid which distilled at 130° C. under 0.2 mbar.

Sources & evidence

ORD record
ord-aea6717286fd4e1997a2c2a882770fbd
Source dataset
uspto-grants-1992_01
Patent number
US05081276

Reaction notes

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