HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dimethyl-4-nitro-I,2-(methylenedioxy)benzene → 2,6-Dimethyl-3,4-(methylenedioxy)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dimethyl-4-nitro-I,2-(methylenedioxy)benzene | HCID 19913822 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2,6-Dimethyl-3,4-(methylenedioxy)aniline | HCID 19913820 | 68% |
Reaction Steps
3,5-Dimethyl-4-nitro-I,2-(methylenedioxy)benzene (5.0 g) and 10% palladium on charcoal catalyst (1.2 g) in ethanol (250 ml) was shaken in a hydrogen atmosphere (50 p.s.i.) at 40° C. for 4 hours. The mixture was filtered through celite and evaporated to leave 2,6-dimethyl-3,4-(methylenedioxy)aniline (2.8 g, 68%) as a dark oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05082848 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-7f37fbeb302c400d979062df539b2ab5 |
| Source note | uspto-grants-1992_01 |