HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Aminophenyl)isoindole-1,3-dione → HCID 178450491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Aminophenyl)isoindole-1,3-dione | HCID 673676 | — |
| Reactant | Ethyl 2-butyryl-3-ethoxyacrylate | HCID 3359484 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 178450491 | HCID 178450491 | — |
Reaction Steps
2-Phthalimidoaniline (44.0 g, 0.21 moles) and ethyl 2-butyryl-3-ethoxyacrylate (45 g, 0.21 moles) were heated together in fusion for 10 minutes then allowed to cool, forming a tan solid. The ethyl 2-buryryl-3-(2-phthalimidophenylamino)acrylate (83.0 g, 97%) was stirred in ether, filtered and dried under vacuum, m.p 153°-5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05082841 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-8929377535d145a9aabccc39fa559cd9 |
| Source note | uspto-grants-1992_01 |