HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorothiophenol → HCID 14650541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorothiophenol | HCID 7815 | — |
| Reactant | Benzyltrimethylammonium hydroxide | HCID 66854 | — |
| Reactant | 2,2-Dimethyl-3,4-epoxy-6-cyanochroman | HCID 10867360 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14650541 | HCID 14650541 | — |
Reaction Steps
A mixture of 2 g of 6-cyano-2,2-dimethyl-3,4-epoxychroman and 1.8 g of parachlorothiophenol in 15 ml of dioxane and 0.3 ml of a 35% methanolic solution of benzyltrimethylammonium hydroxide is refluxed for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05082858 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-f01bdecd7d654596bf956cc6c6285c1e |
| Source note | uspto-grants-1992_01 |