HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexanethiol → HCID 14650546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexanethiol | HCID 15290 | — |
| Reactant | Benzyltrimethylammonium hydroxide | HCID 66854 | — |
| Reactant | 2,2-Dimethyl-3,4-epoxy-6-cyanochroman | HCID 10867360 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 14650546 | HCID 14650546 | — |
Reaction Steps
A mixture of 1.5 g of 6-cyano-2,2-dimethyl-3,4-epoxychroman, 1.2 g of cyclohexylmercaptan and 0.3 g of a 35% methanolic solution of benzyltrimethylammonium hydroxide in 10 ml of tetrahydrofuran is refluxed for 8 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05082858 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-45ff32c47ce04436a3083078524ccafd |
| Source note | uspto-grants-1992_01 |