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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1091020Generated: November 3, 2026

Anthranilamide → 2-[(4-Methoxybenzoyl)carbamothioylamino]benzamide

https://huagongshe.com/reaction/1091020

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAnthranilamideHCID 6942—
Reactant4-Methoxybenzoyl isothiocyanateHCID 140136—
SolventDiethyl EtherHCID 3283—
Product2-[(4-Methoxybenzoyl)carbamothioylamino]benzamideHCID 89281483.3%

Reaction Steps

To a stirred mixture of 7.5 g of 2-aminobenzamide and 150 ml of ether was added dropwise, a mixture of 10 g of 4-methoxybenzoyl isothiocyanate in ether over 15 minutes. After stirring overnight the solid was collected, giving 14.2 g of N-[[[2-(aminocarbonyl)phenyl]amino]thioxomethyl]-4-methoxybenzamide.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05084457
Source datasetuspto-grants-1992_01
ORD IDord-d49142d3b1b5459da5bd74479f17b4d2
Source noteuspto-grants-1992_01