HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilamide → N-[(2-carbamoylphenyl)carbamothioyl]-4-methylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | 4-Methylbenzoyl isothiocyanate | HCID 140139 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-[(2-carbamoylphenyl)carbamothioyl]-4-methylbenzamide | HCID 667640 | 98.2% |
Reaction Steps
To a stirred mixture of 5.4 g of 2-aminobenzamide and 200 ml of ether was added dropwise, a solution of 7.5 g of 4-methylbenzoyl isothiocyanate in 100 ml of ether over 30 minutes. After 48 hours the solid was collected, giving 12.2 g of N-[[[2-(aminocarbonyl)phenyl]amino]thioxomethyl]-4-methylbenzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05084457 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-9ace0fbe23234bbcaa3de7db82457ca0 |
| Source note | uspto-grants-1992_01 |