HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Methylamino)benzamide → m-Toluamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Methylamino)benzamide | HCID 101222 | — |
| Reactant | 3-Methylbenzoyl isothiocyanate | HCID 141397 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | m-Toluamide | HCID 69253 | — |
Reaction Steps
To a stirred mixture of 7.97 g of 2-methylaminobenzamide and 200 ml of ether was added dropwise, a solution of 10 g of 3-methylbenzoyl isothiocyanate in ether over 10 minutes. After 48 hours the solid was collected, giving 15.5 g of N-[[[2-aminocarbonyl)phenyl]methylamino]thioxomethyl]-3-methylbenzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05084457 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-299d1b0de14947dc830a9481a2ef440f |
| Source note | uspto-grants-1992_01 |