Ammonia → HCID 178486916, compound

Participants

Reaction Steps

To a stirred mixture of 5.5 g of the above benzamide, 100 ml of methanolic ammonia and 200 ml of methanol was added dropwise, in increments, 25 ml of 30% hydrogen peroxide. After stirring overnight, the solid was collected, partially dissolved in 600 ml of hot acetonitrile and filtered. The filtrate was chilled, giving 2.4 g of the desired product as white crystals, mp 226°-227° C. (dec.).

Provenance & Evidence