HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl isothiocyanate → HCID 4471447, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl isothiocyanate | HCID 68284 | — |
| Reactant | 2-Amino-N-phenylbenzamide | HCID 78142 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 4471447 | HCID 4471447 | 97.8% |
Reaction Steps
To a stirred mixture of 10 g of 2-amino-N-phenylbenzamide and 500 ml of ether was added dropwise, a solution of 7.7 g of benzoyl isothiocyanate in 100 ml of ether over 20 minutes. After standing several hours the solid was collected, giving 17.3 g of 2-[[(benzoylamino)thioxomethyl]amino]-N-phenylbenzamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05084457 |
| Source dataset | uspto-grants-1992_01 |
| ORD ID | ord-894a7b419f2342aea5763d3d37671532 |
| Source note | uspto-grants-1992_01 |