HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1091168Generated: November 2, 2026
p-Acetylphenyl acetate → Benzenemethanol, 4-(acetyloxy)-alpha-methyl-
https://huagongshe.com/reaction/1091168
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | p-Acetylphenyl acetate | HCID 83063 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Nickel | HCID 935 | — |
| Product | Benzenemethanol, 4-(acetyloxy)-alpha-methyl- | HCID 92345 | 80.4% |
Reaction Steps
102 g of 4-acetoxyacetophenone and 10 g of Raney nickel catalyst are charged in a 300-ml stirred reactor. The reactor is then charged with hydrogen at 500 psig and heated to 60° C. for 270 minutes. The reactor is then cooled down and the product analyzed by gas chromatography. The analysis gives 80.4% 4-acetoxyphenyl methylcarbinol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05084533 |
|---|
| Source dataset | uspto-grants-1992_01 |
|---|
| ORD ID | ord-722b9c64d7f74dcaa6553ccd6814b549 |
|---|
| Source note | uspto-grants-1992_01 |
|---|