HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 66592790, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Reactant | HCID 86636832 | HCID 86636832 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66592790 | HCID 66592790 | — |
Reaction Steps
A mixture of Methyl 3-(2-chlorohydrazino)-4-methoxybenzoate (from step 1) (0.0042 mol) and N-Boc-4-piperidone (0.0063 mol) in ethanol (20 ml) was stirred for 18 h at room temperature. Reaction was concentrated under vacuum and product was isolated with silica gel column chromatography using 20% ethyl acetate in petroleum ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129401B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-4bd72b7474d84a2291ab9dfca1896573 |
| Source note | uspto-grants-2012_03 |