Sodium borohydride → HCID 42636429, compound

Participants

Reaction Steps

Compound 40 was prepared by reduction of (1S,2R,3R,4S,5R,6R)-4-(acetoxymethyl)-6-(3-(4-acetylbenzyl)-4-chlorophenyl)cyclohexane-1,2,3,5-tetrayl tetraacetate (38) with excess sodium borohydride and purification by preparative HPLC to give 0.6 mg of a clear film. MS (ESI+): 445 [M+Na]+, (ESI−): 467 [M+HCOO]−.

Provenance & Evidence