HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66590284, compound → HCID 56849260, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66590284 | HCID 66590284 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 56849260 | HCID 56849260 | 34.4% |
Reaction Steps
9A (50 mg, 64 μmol) was dissolved in 10% trifluoroacetic acid in dichloromethane. The mixture was stirred at room temperature for 2 hours. Solvent was removed under vacuum. The residue was purified by preparatory LCMS (water:acetonitrile, 40-65%) to give Compound 5 (15 mg, 33%). ESI-MS:m/z 679.3 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129538B1 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-b4267df1a57f4b549b728846fb9b1bcb |
| Source note | uspto-grants-2012_03 |