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HRID1092896

反应详情

EQUATION

反应方程式

HRID 1092896 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)[Si](C)(C)OCC(CCl)OC1CCCCO1
HCID23080237

未命名化合物

结构：O=[N+]([O-])c1c[nH]c(Cl)n1
HCID178526855

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)[Si](C)(C)OCC(Cn1cc([N+](=O)[O-])nc1Cl)OC1CCCCO1
HCID66589306

未命名化合物

收率 74.3%

PROCEDURE

实验过程

Similar to Example 28, the objective compound was synthesized from 2-chloro-4-nitroimidazole (2.15 g) and 1-(tert-butyldimethylsilanyloxy)-3-chloro-2-(tetrahydropyran-2-yloxy)propane (12 g), there was obtained 1-[3-(tert-butyldimethylsilanyloxy)-2-(tetrahydropyran-2-yloxy)propyl]-2-chloro-4-nitroimidazole (3.03 g, yield: 74.3%) as colorless liquid product.