HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3-Difluoropiperidine → HCID 123283309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3-Difluoropiperidine | HCID 2758350 | — |
| Reactant | Silanediamine, N,N'-bis(1,1-dimethylethyl)- | HCID 57370846 | — |
| Product | HCID 123283309 | HCID 123283309 | — |
Reaction Steps
A quantity of 0.1 mol 3,3-difluoropiperidine and 0.1 mol bis(t-butylamino)silane were mixed and stirred in a flask under the protection of nitrogen. Every 4 hours, the mixture was pumped with vacuum of 100 torr for 30 minutes. After 48 hours, the end-product bis(3,3-difluoropiperidino)silane was obtained by vacuum distillation at 118° C. / 10 torr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08129555B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-482bc5adc42243259caecc15b0020bc9 |
| Source note | uspto-grants-2012_03 |