Hydrochloric Acid → HCID 66594186, compound

Participants

Reaction Conditions

Reaction Steps

Compound 8-1 (740 mg) was dissolved in ethanol (20 ml), concentrated hydrochloric acid (3 ml) was added, and the mixture was stirred at 80° C. for 2.5 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether to give the object product (540 mg) as a white powder.

Provenance & Evidence