Hydrochloric Acid → HCID 86761511, compound

Participants

Reaction Conditions

Reaction Steps

Compound 12-3 (810 mg) was dissolved in ethanol (20 ml), concentrated hydrochloric acid (2 ml) was added, and the mixture was stirred at 80° C. for 2.5 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether to give the object product (600 mg) as a white powder.

Provenance & Evidence