Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59407837 | HCID 59407837 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66594360 | HCID 66594360 | — |
Reaction Steps
Compound 15-3 (720 mg) was dissolved in ethanol (20 ml), concentrated hydrochloric acid (2 ml) was added, and the mixture was stirred at 80° C. for 2 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether to give the object product (530 mg) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08129361B2 |
|---|
| Source dataset | uspto-grants-2012_03 |
|---|
| ORD ID | ord-102c23e0ea7848c6a48ab82118242408 |
|---|
| Source note | uspto-grants-2012_03 |
|---|
