Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59407955 | HCID 59407955 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66594475 | HCID 66594475 | — |
Reaction Steps
Compound 22-3 (740 mg) was dissolved in ethanol (15 ml), concentrated hydrochloric acid (1.5 ml) was added, and the mixture was stirred at 80° C. for 2.5 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether to give the object product (540 mg) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08129361B2 |
|---|
| Source dataset | uspto-grants-2012_03 |
|---|
| ORD ID | ord-050e854b92aa4494a435b84368aaf316 |
|---|
| Source note | uspto-grants-2012_03 |
|---|
