Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 59407566 | HCID 59407566 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66594031 | HCID 66594031 | 180% |
Reaction Steps
Compound 25-3 (760 mg) was dissolved in ethanol (15 ml), concentrated hydrochloric acid (1.5 ml) was added, and the mixture was stirred at 80° C. for 2 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether to give the object product (560 mg) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08129361B2 |
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| Source dataset | uspto-grants-2012_03 |
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| ORD ID | ord-c2b56e320c314d40a3578a89ecfa67b8 |
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| Source note | uspto-grants-2012_03 |
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