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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1093399Generated: October 31, 2026

Hydrochloric Acid → HCID 66594132, compound

https://huagongshe.com/reaction/1093399

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 59407616HCID 59407616—
SolventEthanolHCID 702—
ProductHCID 66594132HCID 66594132—

Reaction Conditions

Temperature80 °C

Reaction Steps

Compound 49-4 (670 mg) was dissolved in ethanol (15 ml), concentrated hydrochloric acid (1.5 ml) was added, and the mixture was stirred at 80° C. for 1 hr. The reaction mixture was concentrated, and the residue was washed with diethyl ether to give the object product (490 mg) as a white powder.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08129361B2
Source datasetuspto-grants-2012_03
ORD IDord-bb740b2d1ebd414cb56d878dce9a887b
Source noteuspto-grants-2012_03