1,2-Diphenylethylamine → HCID 59353141, compound

HRID 1094059Notes

Reaction equation

HRID 1094059 reaction equation
Br[C:2]1[CH:7]=[CH:6][C:5]([F:8])=[CH:4][C:3]=1[C:9]1[C:18]2[C:17](=[O:19])[N:16]([CH3:20])[C:15](=[O:21])[N:14]([CH3:22])[C:13]=2[N:12]=[C:11](Cl)[C:10]=1[C:24]#[N:25].[C:26]1([CH:32]([NH2:40])[CH2:33][C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1.NCC1C(N2CCOCC2)=NC2N(C)C(=O)N(C)[C:50](=[O:51])C=2C=1C1C=C(F)C=CC=1Br>>[NH2:25][CH2:24][C:10]1[C:11]([NH:40][CH:32]([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)[CH2:33][C:34]2[CH:35]=[CH:36][CH:37]=[CH:38][CH:39]=2)=[N:12][C:13]2[N:14]([CH3:22])[C:15](=[O:21])[N:16]([CH3:20])[C:17](=[O:19])[C:18]=2[C:9]=1[C:3]1[CH:4]=[C:5]([F:8])[CH:6]=[CH:7][C:2]=1[O:51][CH3:50]

Participants

4

Reactant 3

HCID 264821,2-DiphenylethylamineHCID 11605368HCID 11605368, compoundHCID 11683267HCID 11683267, compound

Product 1

HCID 59353141HCID 59353141, compound

Procedure

The title compound was prepared from Compound 47a (Example 42) and 1,2-diphenylethanamine, according to procedure described in the synthesis of Compound 47. MS [m+H] calc'd C32H31FN5O3 540; found 540.

Sources & evidence

ORD record
ord-6ba04d1929074f2589e695140b7da760
Source dataset
uspto-grants-2012_03
Patent number
US08133898B2

Reaction notes

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