HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Propylthiophene-2-carboxylic acid → 2-Ethyl-6-methyl-4-[5-(5-propyl-thiophen-2-yl)-[1,3,4]oxadiazol-2-yl]-phenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Propylthiophene-2-carboxylic acid | HCID 3164314 | — |
| Reactant | 4-Benzyloxy-3-ethyl-5-methyl-benzoic acid hydrazide | HCID 59202026 | — |
| Product | 2-Ethyl-6-methyl-4-[5-(5-propyl-thiophen-2-yl)-[1,3,4]oxadiazol-2-yl]-phenol | HCID 136029939 | — |
Reaction Steps
2-Ethyl-6-methyl-4-[5-(5-propyl-thiophen-2-yl)-[1,3,4]oxadiazol-2-yl]-phenol is prepared in analogy to Example 29 starting from 4-benzyloxy-3-ethyl-5-methyl-benzoic acid hydrazide and 5-propyl-thiophene-2-carboxylic acid; LC-MS: tR=0.99 min, [M+1]+=329.13.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08133910B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-090ca7c5f60e460fb0bd14d6f95763c3 |
| Source note | uspto-grants-2012_03 |