1,2,3-Indantrione, monohydrate → HCID 66636918, compound

HRID 1094335Notes

Reaction equation

HRID 1094335 reaction equation
[CH:1]([NH:4][C:5]1[CH2:10][CH2:9][CH2:8][C:7](=[O:11])[CH:6]=1)([CH3:3])[CH3:2].O.[C:13]1(=[O:24])[C:21]2[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=2)[C:15](=[O:22])[C:14]1=[O:23]>C(Cl)(Cl)Cl>[OH:24][C:13]12[C:21]3[C:16](=[CH:17][CH:18]=[CH:19][CH:20]=3)[C:15](=[O:22])[C:14]1([OH:23])[C:6]1[C:7](=[O:11])[CH2:8][CH2:9][CH2:10][C:5]=1[N:4]2[CH:1]([CH3:3])[CH3:2]

Participants

4

Reactant 2

HCID 2006611,2,3-Indantrione, monohydrateHCID 21625915HCID 21625915, compound

Product 1

HCID 66636918HCID 66636918, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

Equimolar amounts of 3-isopropylaminocyclohex-2-enone and indanetrione hydrate (ninhydrin) were dissolved in chloroform and stirred at room temperature for 12 h. The solvent was then stripped off, and the oily residue was crystallized from acetone.

Workup

  1. customthe oily residue was crystallized from acetone

Sources & evidence

ORD record
ord-64593e6d18e14a538e62f65a6b9e57f2
Source dataset
uspto-grants-2012_03
Patent number
US08133913B2

Reaction notes

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