HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxo(pyridin-3-yl)acetic acid → HCID 58007520, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxo(pyridin-3-yl)acetic acid | HCID 13548099 | — |
| Reactant | HCID 58007505 | HCID 58007505 | — |
| Product | HCID 58007520 | HCID 58007520 | 26.2% |
Reaction Steps
In analogy to example 13, p-tolyl-[2-(6-trifluoromethyl-pyridin-3-yl)-ethyl]-amine (95 mg, 0.34 mmol, prepared as in example 14, step1) was coupled to oxo-pyridin-3-yl-acetic acid (54 mg, 0.36 mmol) and reduced to give the title compound as a colorless oil (37 mg, 25%) MS m/e: 416.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08133909B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-c66dfd970d9548b89b96656d1d4a698e |
| Source note | uspto-grants-2012_03 |