(2S)-2-(((tert-butoxy)carbonyl)amino)-2-phenylacetic acid → HCID 58007560, compound

HRID 1094364Notes

Reaction equation

HRID 1094364 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([NH:9][CH2:10][CH2:11][C:12]2[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=2)[CH:5]=[CH:6][C:7]=1[CH3:8].[CH3:18][C:19]([O:22][C:23]([NH:25][C@H:26]([C:33](O)=[O:34])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)=[O:24])([CH3:21])[CH3:20]>>[C:19]([O:22][C:23](=[O:24])[NH:25][C@H:26]([C:33](=[O:34])[N:9]([C:4]1[CH:5]=[CH:6][C:7]([CH3:8])=[C:2]([CH3:1])[CH:3]=1)[CH2:10][CH2:11][C:12]1[CH:13]=[N:14][CH:15]=[CH:16][CH:17]=1)[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1)([CH3:21])([CH3:18])[CH3:20]

Participants

3

Reactant 2

HCID 11010409(2S)-2-(((tert-butoxy)carbonyl)amino)-2-phenylacetic acidHCID 55169203(3,4-Dimethyl-phenyl)-(2-pyridin-3-yl-ethyl)-amine

Product 1

HCID 58007560HCID 58007560, compound

Procedure

In analogy to the procedure described for the synthesis example 21, step 3, the title compound was prepared from (3,4-dimethyl-phenyl)-(2-pyridin-3-yl-ethyl)-amine and boc-L-alpha-phenylglycine. MS (m/e): 460.3 [M+H]+.

Workup

  1. customIn analogy to the procedure described for the synthesis example 21, step 3

Sources & evidence

ORD record
ord-04f32f3298114c3f8af96f64d37cef1a
Source dataset
uspto-grants-2012_03
Patent number
US08133909B2

Reaction notes

Loading…