HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-1-methoxy-2-methylbenzene → HCID 58007575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-1-methoxy-2-methylbenzene | HCID 608315 | — |
| Reactant | 2-(5-Trifluoromethyl-pyridin-2-YL)-ethylamine | HCID 18071344 | — |
| Product | HCID 58007575 | HCID 58007575 | — |
Reaction Steps
In analogy to the procedure described for the synthesis example 71 (step 1), the title compound (4-methoxy-3-methyl-phenyl)-[2-(5-trifluoromethyl-pyridin-2-yl)-ethyl]-amine (MS m/e: 311.3 [M+H]+) was prepared from 4-bromo-2-methyl-anisole instead of 6-bromo-2,3-dihydro-benzofuran and 2-(5-trifluoromethyl-pyridin-2-yl)-ethylamine instead of 2-(6-trifluoromethyl-pyridin-3-yl)-ethylamine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08133909B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-fea8ba4acbc54bfaa8ad4638f5a1e24b |
| Source note | uspto-grants-2012_03 |