HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1094476Generated: October 30, 2026
Azobisisobutyronitrile → Prop-2-enenitrile--ethenylbenzene (1/1)
https://huagongshe.com/reaction/1094476
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Tricalcium Phosphate | HCID 24456 | — |
| Solvent | Water | HCID 962 | — |
| Product | Prop-2-enenitrile--ethenylbenzene (1/1) | HCID 62696 | — |
Reaction Steps
75 parts by weight of styrene, 25 parts by weight of acrylonitrile, and 120 parts by weight of deionized water are mixed. 0.2 parts by weight of azobisisobutylonitrile (AIBN), 0.4 parts by weight of tricalciumphosphate and 0.2 parts by weight of mercaptan-containing chain transfer agent are added into the mixture. The resultant solution is heated from room temperature to 80° C. for 90 minutes and then kept for 180 minutes at this temperature to obtain a styrene-acrylonitrile copolymer resin (SAN). The styrene-acrylonitrile copolymer resin (SAN) is washed, dehydrated and dried to obtain a styrene-acrylonitrile copolymer resin (SAN) in a powder form. The prepared styrene-acrylonitrile copolymer resin (SAN) has a weight average molecular weight (Mw) of about 90,000 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08133946B2 |
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| Source dataset | uspto-grants-2012_03 |
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| ORD ID | ord-ce784d56a4cf4ce3a7c5ea275c984c28 |
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| Source note | uspto-grants-2012_03 |
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