HCID 66640457, compound → HCID 66640109, compound

Participants

Reaction Steps

As a solution in 25 ml THF, 469 mg (1.04 mMol) 6-benzyloxy-benzooxazole-3-carboxylic acid (4-chloro-3-trifluoromethyl-phenyl)-amide are hydrogenated during 1 h in the presence of 267 mg Pd/C (10%). The catalyst is filtered off, washed with THF and the filtrate concentrated. Trituration with hexane gives the crystalline title compound, which is filtered off and washed with hexane: HPLC: tRet=14.3.

Provenance & Evidence