Ethylamine → N-ethyl-N,N-bis[2-(tert-butoxycarbonylamino)ethyl]amine

HRID 1094677Notes

Reaction equation

[C:1]([O:5][C:6]([NH:8][CH2:9][CH:10]=O)=[O:7])([CH3:4])([CH3:3])[CH3:2].[CH2:12]([NH2:14])[CH3:13]>>[CH2:12]([N:14]([CH2:10][CH2:9][NH:8][C:6]([O:5][C:1]([CH3:2])([CH3:3])[CH3:4])=[O:7])[CH2:10][CH2:9][NH:8][C:6]([O:5][C:1]([CH3:4])([CH3:3])[CH3:2])=[O:7])[CH3:13]

Participants

Reactant 2

HCID 6341Ethylamine

HCID 4247255tert-butyl N-(2-oxoethyl)carbamate

Product 1

HCID 60204726N-ethyl-N,N-bis[2-(tert-butoxycarbonylamino)ethyl]amine

Procedure

The product from Example 14A and ethylamine were processed as described in Example 7B to provide the title compound.

Sources & evidence

ORD record: ord-8ad4939c179c4c528d557c42c2424b2c
Source dataset: uspto-grants-2012_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08133892B2

Reaction notes

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