Acetonitrile → HCID 66637015, compound

HRID 1094818Notes

Reaction equation

HRID 1094818 reaction equation
[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[OH:8].BrC[CH2:11][CH2:12][O:13][CH3:14].[C:15](#N)C>>[Br:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[O:8][CH2:11][CH:12]([O:13][CH3:14])[CH3:15]

Participants

4

Reactant 3

HCID 6342AcetonitrileHCID 72442-BromophenolHCID 5245511-Bromo-3-methoxypropane

Product 1

HCID 66637015HCID 66637015, compoundYield 101%

Procedure

2-Bromophenol (861 mg, 4.97 mmol) and 1-bromo-3-methoxypropane (1000 mg, 6.53 mmol) in acetonitrile (10 ml) was treated as for preparation 62 to afford crude title compound as a colourless liquid (1.23 g, 101%).

Sources & evidence

ORD record
ord-66b8c7ead8c741e792470ead6f88994c
Source dataset
uspto-grants-2012_03
Patent number
US08134007B2

Reaction notes

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