HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Acetamidobenzoic acid → 4-acetylamino-N-[4-methyl-5-(2-nitrooxy-ethyl)-thiazol-2-yl]-benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Acetamidobenzoic acid | HCID 19266 | — |
| Reactant | 4-Methyl-5-(2-nitrooxy-ethyl)-thiazol-2-ylamine | HCID 11557499 | — |
| Product | 4-acetylamino-N-[4-methyl-5-(2-nitrooxy-ethyl)-thiazol-2-yl]-benzamide | HCID 18440859 | 44% |
Reaction Steps
Pet-157 was prepared according to the general procedure described hereinabove and the procedure described above for the preparation of Pet-154, using 4-acetylamino-benzoic acid and 4-methyl-5-(2-nitrooxy-ethyl)-thiazol-2-ylamine (Pet-10) as the starting materials, in an overall yield of 44%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134010B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-27c65976fe7240ffb2133f55a9fd21d4 |
| Source note | uspto-grants-2012_03 |