HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Acrylamido-2-methyl-1-propanesulfonic acid → Ammonium acryloyldimethyltaurate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Acrylamido-2-methyl-1-propanesulfonic acid | HCID 65360 | — |
| Reactant | Ethanamine, 2-(2-methoxyethoxy)-N,N-bis[2-(2-methoxyethoxy)ethyl]- | HCID 112414 | — |
| Product | Ammonium acryloyldimethyltaurate | HCID 6850854 | 99% |
Reaction Steps
A nitrogen purged 50 ml schlenk flask was charged with freshly distilled tris[2-(2-methoxyethoxy)-ethyl]amine (1.69 g, 5.24 mmol) and 2-acrylamido-2-methyl-1-propanesulfonic acid (1.09 g, 5.24 mmol) and stirred at ambient temperature for 8 hr or until completely dissolved. Total dissolution completes formation of the AMPS ammonium salt monomer as a transparent light amber oil in a 99% yield which was used immediately without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134024B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-f3d5db68fd8a4c70a4ffb95307229953 |
| Source note | uspto-grants-2012_03 |