HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57675121, compound → HCID 16723095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57675121 | HCID 57675121 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 16723095 | HCID 16723095 | — |
Reaction Steps
Intermediate 47 (0.2 g, 0.32 mmol) was diluted with DCM (10 mL) and treated with TEA (0.3 mL). After 3 h, reaction solvents removed and resulting residue was purified by HPLC (0.01 g, 6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08133900B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-9207e83252bc419e803e12e038a8bd22 |
| Source note | uspto-grants-2012_03 |