HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 5-fluoro-2-{4-[2-(tert-butyl-dimethyl-silanyloxy)ethoxy]-Phenoxy}-benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,4-Difluorobenzaldehyde | HCID 73770 | — |
| Reactant | 4-[2-(Tert-butyl-dimethyl-silanyloxy)-ethoxy]-phenol | HCID 22033378 | — |
| Product | 5-fluoro-2-{4-[2-(tert-butyl-dimethyl-silanyloxy)ethoxy]-Phenoxy}-benzaldehyde | HCID 57743218 | — |
Reaction Steps
In a similar manner to the method described in Example 140a, 2,4-difluoro-benzaldehyde (Aldrich) reacted with 4-[2-(tert-butyl-dimethyl-silanyloxy)-ethoxy]-phenol and potassium carbonate to give a light brown oil which solidifies on standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08134001B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-aca7c439b99e47d68b3349e01e4e3c81 |
| Source note | uspto-grants-2012_03 |