HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-4-(methoxycarbonyl)benzeneboronic acid → HCID 72310556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-4-(methoxycarbonyl)benzeneboronic acid | HCID 23005335 | — |
| Reactant | HCID 66699206 | HCID 66699206 | — |
| Catalyst | Cupric acetate | HCID 8895 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 72310556 | HCID 72310556 | — |
Reaction Steps
In analogy to Example 151, step 8, 3-chloro-5-[2-(2-chloro-4-hydroxy-phenyl)-1-hydroxy-1-trifluoromethyl-propyl]-1-methyl-1H-pyridin-2-one was reacted with 3-chloro-4-methoxycarbonylphenylboronic acid, copper-(II)-acetate and pyridine to give the title compound as a colorless foam. MS (m/e)=564.1 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138189B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-4399936674634eb99d18fc5d9b4e1c78 |
| Source note | uspto-grants-2012_03 |