HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1096779Generated: October 30, 2026
HCID 178422427, compound → HCID 178422426, compound
https://huagongshe.com/reaction/1096779
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 178422427 | HCID 178422427 | — |
| Solvent | 1,1'-Biphenyl, mixt. with 1,1'-oxybis(benzene) | HCID 24670 | — |
| Product | HCID 178422426 | HCID 178422426 | 95% |
Reaction Steps
A mixture of 6-bromo-4-hydroxy-8-methyl-3-quinolinecarboxylic acid (1.80 g, 6.36 mmol) and Dowtherm A (10 mL) was heated at 260° C. for 1.0 h. The reaction was cooled, triturated with hexanes, filtered and dried in a Buchner funnel to give the title compound (1.43 g, 95%) as a tan solid. MS(ES)+ m/e 238 [M+H].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08138347B2 |
|---|
| Source dataset | uspto-grants-2012_03 |
|---|
| ORD ID | ord-87e86cdc389643a48c6a33b2346c2ae8 |
|---|
| Source note | uspto-grants-2012_03 |
|---|
