HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 16723095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 57675121 | HCID 57675121 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 16723095 | HCID 16723095 | — |
Reaction Steps
Intermediate 47 (0.2 g, 0.32 mmol) was diluted with DCM (10 mL) and treated with TFA (0.3 mL). After 3 h, reaction solvents removed and resulting residue was purified by HPLC (0.01 g, 6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08138199B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-66e27ef462c440b1ac588c62ddc6360f |
| Source note | uspto-grants-2012_03 |