HuagongsheHuagongshe Chemistry Print Report · For research reference only
CHEBI:5834 → Acurea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | CHEBI:5834 | HCID 441298 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | Acurea | HCID 3662 | — |
Reaction Steps
2 g of hyperforin (M. W. =536,01) are dissolved in 20 ml of THF under magnetic stirring; the solution is added with LiAlH4 in strong excess (1 g, 0.026 mol, M. W.=38). The progress of the reaction is monitored by TLC (eluent petroleum ether/EtOAc 9:1). After ten minutes the reaction is completed.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE043280E1 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-5c41414fca4e4c35a84c067f7dcd1a5c |
| Source note | uspto-grants-2012_03 |