Thenyl mercaptan → HCID 66814086, compound

HRID 1097356Notes

Reaction equation

HRID 1097356 reaction equation
[OH:1][CH2:2][C@H:3]([NH:5][C:6]1[C:7]2[S:24][C:23](=[O:25])[NH:22][C:8]=2[N:9]=[C:10]([S:12]([CH2:15][C:16]2C=C[CH:19]=[CH:18][CH:17]=2)(=O)=O)[N:11]=1)[CH3:4].[S:26]1C=CC=C1CS>>[OH:1][CH2:2][C@H:3]([NH:5][C:6]1[C:7]2[S:24][C:23](=[O:25])[NH:22][C:8]=2[N:9]=[C:10]([S:12][CH2:15][C:16]2[S:26][CH:19]=[CH:18][CH:17]=2)[N:11]=1)[CH3:4]

Participants

3

Reactant 2

HCID 80408Thenyl mercaptanHCID 66813749HCID 66813749, compound

Product 1

HCID 66814086HCID 66814086, compoundYield 3%

Procedure

The title compound was prepared by the method described in example 16 step b) from the product of example 15 step e) (0.300 g, 0.79 mmol) and 2-thiophenemethanethiol (0.32 ml, 3.9 mmol).

Sources & evidence

ORD record
ord-10bc88b0ff5b466eae5d49f0344bac27
Source dataset
uspto-grants-2012_03
Patent number
US08143261B2

Reaction notes

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