HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pentyn-1-ol → 3-[3-(Phenylmethyl)-5-isoxazolyl]-1-propanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pentyn-1-ol | HCID 79346 | — |
| Reactant | 4-(3-Phenyl-5-isoxazolyl)-1-butanol | HCID 59395604 | — |
| Reactant | HCID 73177631 | HCID 73177631 | — |
| Product | 3-[3-(Phenylmethyl)-5-isoxazolyl]-1-propanol | HCID 58478097 | — |
Reaction Steps
Synthesised as with 4-(3-phenyl-5-isoxazolyl)-1-butanol, using N-hydroxy-2-phenylethanimidoyl chloride (253 mg, 1.5 mmol) and 4-pentyn-1-ol (139 mg, 1.65 mmol). Yield 61 mg of pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143264B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-233cb81c10c7444484fb4459de6ed829 |
| Source note | uspto-grants-2012_03 |