N-Methylisobutylamine → HCID 25116532, compound

HRID 1099436Notes

Reaction equation

HRID 1099436 reaction equation
C[O:2][C:3]([C:5]1[CH:6]=[CH:7][C:8]([C:11]([OH:13])=O)=[N:9][CH:10]=1)=[O:4].[CH3:14][NH:15][CH2:16][CH:17]([CH3:19])[CH3:18]>>[CH2:16]([N:15]([CH3:14])[C:11]([C:8]1[CH:7]=[CH:6][C:5]([C:3]([OH:2])=[O:4])=[CH:10][N:9]=1)=[O:13])[CH:17]([CH3:19])[CH3:18]

Participants

3

Reactant 2

HCID 12249N-MethylisobutylamineHCID 3149925-(Methoxycarbonyl)pyridine-2-carboxylic acid

Product 1

HCID 25116532HCID 25116532, compoundYield 75%

Procedure

The title compound was synthesized as described for Intermediate example I-94 in 75% yield starting from 5-(methoxycarbonyl)pyridine-2-carboxylic acid and n-methylisobutylamine; MS (APPI/APCI) m/z 237[M+H+].

Sources & evidence

ORD record
ord-06fb883d21544528abb1221d789dba7d
Source dataset
uspto-grants-2012_03
Patent number
US08143408B2

Reaction notes

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