HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenoxyethanol → N-[4-(2-Phenoxyethoxy)benzoyl]glycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenoxyethanol | HCID 31236 | — |
| Reactant | N-(4-Hydroxybenzoyl)glycine tert-butyl ester | HCID 10682169 | — |
| Product | N-[4-(2-Phenoxyethoxy)benzoyl]glycine | HCID 66812499 | 78% |
Reaction Steps
The same reaction as in Example 1 (1b) was conducted using N-(4-hydroxybenzoyl)glycine tert-butyl ester (249 mg, 0.991 mmol) prepared in Example 1 (1a) and 2-phenoxyethanol (163 μL, 1.19 mmol) to give 241 mg of the title compound (white powder, yield: 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08143446B2 |
| Source dataset | uspto-grants-2012_03 |
| ORD ID | ord-7f31953755824b4bae656bd26796b2bf |
| Source note | uspto-grants-2012_03 |