化工社化工社 化学情報印刷レポート · 研究参考用
4-Methylphenethyl alcohol → N-{4-[2-(4-Methylphenyl)ethoxy]benzoyl}glycine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Methylphenethyl alcohol | HCID 95294 | — |
| 反応物 | N-(4-Hydroxybenzoyl)glycine tert-butyl ester | HCID 10682169 | — |
| 生成物 | N-{4-[2-(4-Methylphenyl)ethoxy]benzoyl}glycine | HCID 66811767 | 90% |
反応手順
The same reaction as in Example 1 (1b) was conducted using N-(4-hydroxybenzoyl)glycine tert-butyl ester (275 mg, 1.09 mmol) prepared in Example 1 (1a) and 2-(4-methylphenyl)ethanol (159 μL, 1.14 mmol) to give 306 mg of the title compound (colorless crystalline solid, yield: 90%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08143446B2 |
| 出典データセット | uspto-grants-2012_03 |
| ORD ID | ord-49b8f8009fe64dccb7496751d46bb7ef |
| 出典メモ | uspto-grants-2012_03 |