5-Bromonicotinic acid → Methyl 3-{N-[(5-bromopyridin-3-yl)carbonyl]-S-methylsulfonimidoyl}benzoate

HRID 1099687Notes

Reaction equation

HRID 1099687 reaction equation
[Br:1][C:2]1[CH:3]=[N:4][CH:5]=[C:6]([CH:10]=1)[C:7]([OH:9])=O.[CH3:11][S:12]([C:15]1[CH:16]=[C:17]([CH:22]=[CH:23][CH:24]=1)[C:18]([O:20][CH3:21])=[O:19])(=[NH:14])=[O:13]>>[Br:1][C:2]1[CH:10]=[C:6]([C:7]([N:14]=[S:12]([C:15]2[CH:16]=[C:17]([CH:22]=[CH:23][CH:24]=2)[C:18]([O:20][CH3:21])=[O:19])([CH3:11])=[O:13])=[O:9])[CH:5]=[N:4][CH:3]=1

Participants

3

Reactant 2

HCID 887075-Bromonicotinic acidHCID 57657957Methyl 3-[imino(methyl)oxo-lambda6-sulfanyl]benzoate

Product 1

HCID 57657891Methyl 3-{N-[(5-bromopyridin-3-yl)carbonyl]-S-methylsulfonimidoyl}benzoate

Procedure

In a manner similar to that described in Example 480 (step 6), 5-bromonicotinic acid and methyl 3-(S-methylsulfonimidoyl)benzoate were reacted to give the title compound.

Workup

  1. customwere reacted

Sources & evidence

ORD record
ord-a263eaf5c71f402f942defc5b1961f68
Source dataset
uspto-grants-2012_03
Patent number
US08143410B2

Reaction notes

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